不同压力下气层岩样m、n值变化的实验研究

胶结指数m和饱和度指数n变化规律的研究一直是岩石物理学家和测井解释分析家关注的问题。压力是影响m、n的重要因素,但迄今为止,仍未取得可使多数人接受的一般性结论。实验开展了低孔隙度低渗透率气层岩样在不同压力条件下的电阻率测量,在考虑孔隙度随压力变化的基础上建立了m、n参数随压力变化的关系,得出结论:某些地区的气层岩样在压力增大时即使考虑孔隙度变化,m值增大,n值减小。     

东营凹陷古近系砂岩储集层特征对比

东营凹陷可分为北部陡坡带、中央隆起带和南部缓坡带，由于地质背景有差异，古近系砂岩储集层在不同地区的特征不同：北部陡坡带以近岸水下扇砂砾岩沉积为主，进入晚成岩期的时间早，深度浅，次生孔隙发育中等，主要分布在1650-2450m深度，3200-3500m深度存在第二次生孔隙带，碳酸盐溶蚀和胶结作用在垂向具有分带性；中央隆起带以浊积扇砂岩为主，但由于断裂发育，酸性水活跃，进入晚成岩期的时间也较早，次生孔隙最发育，又分布范围大，1800-3500m深度均发育次生孔隙，碳酸盐胶结弱，储集层物性最好；南部缓坡带以滨浅湖和三角洲沉积为主，进入晚成岩期的时间晚，次生孔隙发育少，北部和中部物性相对差。图4表1参31     

UCT测井技术在河南油田的应用

介绍了超声波固井质量检测仪(UCT)的原理、结构及测井方法，分析了UCT测井资料的应用情况。实践表明，UCT能准确地探测套管腐蚀，直观评价水泥与套管、水泥与地层一、二界面的胶结质量。     

Simultaneous chromizing-aluminizing coating of austenitic stainless steels

Chromium and aluminum were simultaneously co-deposited by diffusion into austenitic stainless steel substrates, by a single-step, pack-cementation process. The mechanism for the formation of diffusion-coated products on 304 and 316 stainless steels and on Incoloy 800 is discussed. The morphologies of the phases formed at the surface, i.e., an external beta layer and an underlying multiphase interdiffusion zone, are presented. The formation of the brittle, , outer layer was minimized by variations in the pack composition and activator. The coated 304 and 316 steels exhibited excellent scaling resistance upon oxidation in air at 1000°C.     

Codeposited chromium and silicon diffusion coatings for Fe-Base alloys via pack cementation

The simultaneous deposition of Cr and Si into plain carbon, low-alloy, and austenitic steels using a halide-activated pack-cementation process is described. Equilibrium partial pressures of gaseous species have been calculated using the STEPSOL computer program to aid in designing specific processes for codepositing the desired ratios of Cr and Si into a given alloy. The calculations indicate that NaCl-activated packs are chromizing, while NaF-activated packs deposit more Si with less Cr. The use of a dual activator (e.g., NaF+NaCl) allows for the deposition of both Cr and Si in the desired amounts. Single-phase ferritic coatings (150–250 microns thick) with a surface concentration of 20–35 wt.% Cr and 2–4% Si have been grown on AISI 1018, Fe-2.25 Cr-1.0Mo-0.15C, and Fe-0.5 Cr-0.5 Mo-0.2C steels using packs containing a 90 wt.% Cr-10Si binary source alloy, a NaF+NaCl activator, and a silica filler. Two-phase coatings (approximately 75 microns thick) containing 20–25 wt.% Cr and 2.0–2.4% Si have been obtained on 304 stainless steel using packs containing a 90 wt.% Cr-10Si binary source alloy, a NaF activator, and an alumina filler. The same pack chemistry allowed the diffusion of Cr and Si into the austenitic Incoloy 800 alloy without a phase change. A coated Fe-2.25 Cr-1.0 Mo-0.15 C coupon with a surface concentration of Fe-34 wt.% Cr-3Si was cyclically oxidized in air at 700°C for over four months and 47 cycles. The weight gain was very low (<0.2 mg/cm²) with no scale spalling detected. Coated coupons of AISI 1018 steel, and Fe-0.5 Cr-0.5 Mo-0.2C steel have shown excellent oxidation-sulfidation resistance in reducing, sulfur-containing atmospheres at temperatures from 400 to 700°C and in erosion and erosion-oxidation testing in air at 650 and 850°C.     

空气-乙炔碳氮氧离子多元共渗工艺研究

用空气-乙炔混合气体作为气源,对40Cr钢进行了离子碳氮氧多元共渗;用光学金相显微镜、X射线衍射仪和显微硬度计,对渗层形貌、物相和显微硬度进行了分析检测。结果表明:乙炔浓度是影响性能的关键因素,它对硬度、物相起着决定性的作用。与常规离子渗氮相比,以空气-乙炔混合气体作为气源的碳氮氧离子多元共渗工艺操作简便,成本低廉。     

高锗锌原料湿法冶炼的实践

分析了锗在湿法炼锌浸出—净化过程中的行为,并通过实践确定了高锗锌原料湿法处理的工艺条件,介绍了存在的问题和解决措施。     

炭/炭复合材料MoSi2/SiC抗氧化涂层的研究

采用包埋法制备C／C复合材料抗氧化MoSi2／SiC梯度涂层，同时对抗氧化涂层的形成、组织结构以及抗氧化性能与渗料的关系和抗氧化机理进行了研究。结果表明：采用包埋法制备的C／C复合材料抗氧化MoSi2／SiC梯度涂层致密，但有少量裂纹，涂层有良好的抗氧化效果。当硅与SiC保持一定的比例，渗料中MoSi2的含量为50％时，涂层具有最好的抗氧化效果；当MoSi2与SiC保持一定的比例，渗料中硅的含量为20％时，涂层具有最好的抗氧化效果。     

铜基镀镍料浆包渗铬层组织和性能研究

硬度低和耐磨性较差制约了铜在冶金设备领域的应用.为了提高铜金属表面硬度和耐磨性,采用镀镍料浆包渗铬技术对铜表面进行渗铬.制备渗铬层,并对其微观组织、扩散特性及显微硬度和耐磨性进行了研究.结果表明:铜表面经镀镍渗铬处理后,在镍层表面获得50μm的渗铬层,渗层组织为镍铬固溶体相;渗层硬度由外层的345 HV逐渐降低到镍镀层的120 HV和铜基体的70 HV,渗层显微硬度随铬含量的降低而降低.渗铬处理将铜和镍的摩擦系数由原来的0.8和0.6降低到0.45.